Robert Jacobson

X-Ray Crystallography and Molecular Mechanics Methods

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Selected Publications

  1. Jacobson, R. A. and Lipscomb, W. N., "The B8C18 Structure: A New Polyhedron in Small Molecules", J. Am. Chem. Soc. 80, 5571 (1958).
  2. Jacobson, R. A. and Lipscomb, W. N., "Molecular and Crystal Structure of B8C18 II. Solution of the Three-Dimensional Structure", J. Chem. Phys. 31, 605 (1959).
  3. Rossmann, M. G., Jacobson, R. A., Hirshfeld, F. L., and Lipscomb, W. N., "An Account of Some Computing Experiences", Acta Cryst. 12, 530 (1959).
  4. Jacobson, R. A., Wunderlock, J. A., and Lipscomb, W. N., "Structure of Cellobiose", Nature 184, 1719 (1959).
  5. Jacobson, R. A., Wunderlich, J. A., and Lipscomb, W. N., "The Crystal and Molecular Structure of Cellobiose", Acta Cryst. 14, 598 (1961).
  6. Jacobson, R. A., Penfold, B. R., and Lipscomb, W. N., "A Superposition Method and Program for Image-Seeking Procedures in Crystallography" as part of book entitled "Computing Methods and the Phase Problem in X-rays Crystal Structure Analysis, edited by R. Pepinsky, J. M. Robertson and J. C. Speakman. Pergamon Press, Inc., New York, 1961, 326 pp.
  7. Goldstein, P. and Jacobson, R. A., "Structure of Dimethyl Phosphinoborine Tetramer", J. Amer. Chem. Soc. 84, 2457 (1962).
  8. Mighell, A. D. and Jacobson, R. A., "Analysis of Three-Dimensional Patterson Maps Using Vector Verification", Acta Cryst. 16, 443 (1963).
  9. Gorres, B. T. and Jacobson, R. A., "The Use of Frequency Check in the Vector Verification Method", Acta Cryst. 17, 1599 (1964).
  10. Mighell, A. D. and Jacobson, R. A., "The Crystal Structure of 3,3,4,4-Tetrahydrofurantetrol [An Application of Vector Verification]", Acta Cryst. 17, 1554 (1964).
  11. Wilkes, C. E. and Jacobson, R. A., "The Crystal Structure of Di-µ- diphenylphosphinatoacetylacetonatochromium[III]", Inorg. Chem. 4, 99 (1965).
  12. Jacobson, R. A. and Guggenberger, L. J., "Weighting Factors in Image-Seeking Methods", Acta Cryst. 20, 592 (1966).
  13. Schlueter, A. W., Jacobson, R. A., and Rundle, R. E., "A Redetermination of the Crystal Structure of CsCuC13", Inorg. Chem. 5, 277 (1966).
  14. Lawton, S. L. and Jacobson, R. A., "Crystal Structure Studies of Some Unusual Antimony Bromide Salts", J. Amer. Chem. Soc. 88, 616 (1966).
  15. Lawton, S. L. and Jacobson, R. A., "The Crystal Structure of Ammonium Hexabromoantimonate, (NH4)4SbIIISbVBr12", Inorg. Chem. 5, 743 (1966).
  16. Hoard, L. G. and Jacobson, R. A., "The Structure of N-Methyltrichlorophosphinimine Dimer", J Chem. Soc. A, 1966, 1203.
  17. Hansen, P. J. and Jacobson, R. A., "Crystal Structure Determination of π-C5H5Fe(CO)2Mn(CO)5M", J. Organomet. Chem. 6, 389 (1966).
  18. Schlueter, A. W. and Jacobson, R. A., "The Structure of (NPC12)5 A Ten-Membered Phosphorus-Nitrogen Ring', J. Amer. Chem. Soc. 88, 2051 (1966).
  19. Dahm, D. J. and Jacobson, R. A., "The Probable Molecular Configuration of Fe3(CO)12 Based on the Structure of Fe3(CO)11PPh3", Chem. Comm. 15, 496 (1966).
  20. Mighell, A. D. and Jacobson, R. A., "Use of the Consistency Check in the Vector Verification Method", J. Research, NBS, 70A, 4 (July-Aug. 1966).
  21. Jacobson, R. A., "On the Use of Weights and Symmetry in the Superposition Procedure", Transactions of the American Crystallographic Association, 2, 1966. (Proceedings of the Symposium on Machine Interpretations of Patterson Functions and Alternative Direct Approaches and the Austin Symposium on Gas Phase Molecular Structure.
  22. Porter, S. K. and Jacobson, R. A., "The Preparation and Crystal Structure Determination of Pyridinium Tetrachloroantimonate(III),
  23. 1244 (1967). 23. Chipman, D. M. and Jacobson, R. A., "The Crystal Structure of cis-N-Methylcarboxamido Methylamine Tetracarbonyl Manganese(I) Mn(CO)4(NH2CH3)(CONCH3)", Inorg. Chim. Acta 1, 393 (1967).
  24. Schlueter, A. W. and Jacobson, R. A., "The Crystal Structure of (PNC12)5", J. Chem. Soc. 26A, 2317 (1968).
  25. Granoff, B. and Jacobson, R. A., "The Crystal Structure of Dicarbonyl-πcyclopentdienylbicyclo[2.2.1]hepta-2π, 5-dienemanganese(I), (C5H5)Mn(C7H8)(CO)2", Inorg. Chem. 7, 2328 (1968).
  26. Lawton, S. L. and Jacobson, R. A., "The Crystal Structure of - Picolinium Nonabromeantimonate(V), (C6H7NH)2SBVBr9", Inorg. Chem. 7, 2124 (1968).
  27. Guggenberger, L. J. and Jacobson, R. A., "The Crystal Structure of Thorium Diiodide", Inorg Chem. 7, 2328 (1968).
  28. Dahm, D. J. and Jacobson, R. A., "The Crystal Structure of Fe3(CO)11-P(C6H5)3", J. Amer. Chem. Soc. 90, 5106 (1968).
  29. Schlueter, A. W. and Jacobson, R. A., "The Crystal Structure of Azulene Dimolybdenum Hexacarbonyl", Inorganica Chemica Acta 2, 241 (1968).
  30. Guggenberger, L. J. and Jacobson, R. A., "The Crystal Structure of a Benzocyclopropapyran", Acta Cryst. B25, 888 (1969).
  31. Breneman, G. L., Chipman, D. M., Galles, C. J., and Jacobson, R. A., "The Crystal Structure of the Monoclinic Form of Mn(CO)4(NH2CH3)(CONHCH3)", Inorganica Chimica Acta 3, 447 (1969).
  32. Hackert, M. L., Lawton, S. L., and Jacobson, R. A., "Properties of Intervalence Antimony Bromides", Proc. Iowa Acad. Soc. 75, 97 (1968).
  33. Hubbard, C. R. and Jacobson, R. A., "The Crystal Structure of Rb4SIIISbVBr12", Proc. Iowa Acad. Sci. 75, 85 (1968).
  34. Porter, S. K. and Jacobson, R. A., "The Crystal Structure of Pyridinium Tetrachloroantimonate(III)", J. Chem. Soc. (A), 1356 (1970).
  35. Porter, S. K. and Jacobson, R. A., "The Crystal Structure of Pyridinium Nonabromodiantimonate(III) Dibromide", J. Chem. Soc. (A), 1359 (1970).
  36. Hackert, M. L. and Jacobson, R. A., "Conformation of the Inhibitor 1,5-Gluconolactone - An X-Ray Determination", Chem. Comm., 1179 (1969).
  37. Thaxton, C. B. and Jacobson, R. A., "A Technique for Cooling Single Crystals below 90 K for X-Ray Diffraction", Journal of Physics, Series E, 245 (1970).
  38. Martin, D. S., Jr., Jacobson, R. A., Hunter, L. D., and Benson, J. E., "Polarized Absorption Spectra for Single Crystals of Dichloro(ethylenediamine)platinum(II). Effect of Metal-Metal Interactions", Inorg. Chem. 9, 1276 (1970).
  39. Jacobson, R. A., "Patterson Analysis of Superpositions, Symmetry and Peak Evaluations", Crystallographic Computing, F. R. Ahmed, Ed., Munksgaard, Copenhagen, Denmark (1970) pp 81-86.
  40. Hackert, M. L. and Jacobson, R. A., "A Method of Partial Structure Evaluation", Acta Cryst. B26, 1682 (1970).
  41. Rodgers, J. and Jacobson, R. A., "The Crystal and Molecular Structure of the Five-Coordinate Complex Dibromo-[6,6'-dimethylamine-NNN]-Nickel(III)", J. Chem. Soc. (A), 1826 (1970).
  42. Reidel, E. F. and Jacobson, R. A., "The Crystal Structure of a Pentakis (Alkyl Phosphite) Nickel(II) Perchlorate, Ni(PO3C6H9)5(C104)2", Inorg. Chim. Acta 4, 407 (1970).
  43. Ozbirn, W. P. and Jacobson, R. A., "The Crystal and Molecular Structure of the Perchlorate and Chloride of [(NH3)5(CN)Co(III)], Inorg. Chim. Acta 4, 377 (1970).
  44. Hackert, M. L. and Jacobson, R. A., "The Crystal and Molecular Structure of the Inhibitor D-glucono-(1-5)-lactone", Acta Cryst. B27, 203 (1971).
  45. Hackert, M. L. and Jacobson, R. A., "The Crystal Structure of Tetraethylammonium Hexabromoantimonate(V), (C2sH5)4NSbBr6", Inorg. Chem. 10, 1075 (1971).
  46. Hackert, M. L. and Jacobson, R. A., "The Preparation and Crystal Structure of 4-Ethylpyridinium Tetrobromoferrate(III)", Acta Cryst. B27, 1658 (1971).
  47. Hackert, M. L. and Jacobson, R. A., "The Structure of Silver Chromate", J. Solid State Chem. 3, 364 (1971).
  48. Johnson, J. E., Beineke, T. A., and Jacobson, R. A., "The Crystal and Molecular Structure of Bis-(2,2'Dipyridylamine)Copper(II) Perchlorate", J. Chem. Soc. (A) 580 (1971).
  49. Thaxton, C. B. and Jacobson, R. A., "The Crystal Structure of H2Ta6C118·6H2O", Inorg. Chem. 10, 1460 (1971).
  50. Lawton, S. L. and Jacobson, R. A., "The Crystal Structure of Quinuclidinium Dodecabromoantimonate(III,V)-2-Dibromine, (C7H13NH)4SbIIISbVBr24", Inorg. Chem. 10, 709 (1971).
  51. Lawton, S. L., Jacobson, R. A., and Frye, R. S., "The Crystal Structure of Pyridinium Tetracosabromoantimon(III)triantimon(V)ate, (C55NH)6SbIIISbV3Br24", Inorg. Chem. 10, 701 (1971).
  52. Hubbard, C. R. and Jacobson, R. A., "A System of Programs for Generalized Superpositions", J. Appl. Cryst. 3, 549 (1970).
  53. Martin, L. L. and Jacobson, R. A., "The Crystal and Molecular Structure of cis-Dichloro-bis(dimethyl-phenylphosphine)palladium(II)", Inorg. Chem. 10, 1795 (1971).
  54. Hubbard, C. R., Quicksall, C., and Jacobson, R. A., "A New Technique for Neutron Diffraction -- Use of White Radiation", Nucl. Instrum. and Methods, 94, 185 (1971).
  55. Ozbirn, W. P., Jacobson, R. A., and Clardy, J. C., "The Crystal and Molecular Structure of 1,2,5-Triphenylphosphole", Chem. Comm., 1062, (1971).
  56. Clardy, J. C., Hauser, F. M., Dahm, D., Jacobson, R. A., and Wildman, W. C., "Molecular Structure and Absolute Configuration of Alkaloids Related to 5,10-Ethanophenthridine", J. Amer. Chem. Soc. 92, 6337 (1970).
  57. Hubbard, C. R., Quicksall, C. O., and Jacobson, R. A., "A Highly Efficient Neutron Diffraction Technique -- Use of White Radiation", Acta Cryst. A28, 236 (1972).
  58. Martin, L. L. and Jacobson, R. A., "The Crystal and Molecular Structure of Nitrilotriacetodiaquopraseodymium(III) Monohydrate", Inorg. Chem. 11, 2785 (1972).
  59. Martin, L. L. and Jacobson, R. A., "The Crystal and Molecular Structure of Nitrolotriacetodiaquodysprosium(III)-dihydrate", Inorg. Chem. 11, 2789 (1972).
  60. Bowers, R. H., Banks, C. V., and Jacobson, R. A., "A Redetermination of the Crystal and Molecular Structure of Nickel(II) Ethylmethylglyoxime", Acta Cryst. B28, 2318 (1972).
  61. Hubbard, C. R., Quicksall, C. O., and Jacobson, R. A., "A Comparison of Fast Fourier and Trigonometric Fourier Algorithms", J. Appl. Cryst. 5, 234 (1972).
  62. Hubbard, C. R. and Jacobson, R. A., "Molecular Bromine Bridging of SbIII2Br93- Anions and the Crystal Structure of Tetramethylammonium Nonabromodiantimonate(III)- Dibromine", Inorg. Chem. 11, 2247 (1972).
  63. Lipscomb, W. N. and Jacobson, R. A., "X-Ray Crystal Structure Analysis", Physical Methods of Chemistry, Part III D, Ed. by A. Weissberger and B. W. Rossiter, 1972 (pp 1- 124).
  64. Wismer, R. K. and Jacobson, R. A., "PSST: A Combination of Patterson Superposition and Sigma-2 Techniques for Phase Determination", Acta Cryst. B28, 3457 (1972).
  65. Schroeder, D. R. and Jacobson, R. A., "The Crystal Structure of Hexamminecobalt Hexachloroantimonate(III)", Inorg. Chem. 12, 210 (1973).
  66. Schroeder, D. R. and Jacobson, R. A., "The Crystal Structure of Hexamminecobalt Nonaflouroantimonate(III)", Inorg. Chem. 12, 515 (1973).
  67. Porter, S. K. and Jacobson, R. A., "Pyridinium Hexachloroantimonate(V), C5NH6SbC16", Cryst. Structure Comm. 1, 431 (1972).
  68. Johnson, J. E. and Jacobson, R. A., "The Crystal and Molecular Structure of 2,2'Bipyridylamine", Acta Cryst. B29, 1669 (1973).
  69. Gress, M. E. and Jacobson, R. A., "Crystal and Molecular Structure of π- C5H5Fe(CO)3PF6, A Cationic Iron Carbonyl Complex", Inorg. Chem. 12, 1746 (1973).
  70. Johnson, J. E. and Jacobson, R. A., "Crystal and Molecular Structure of Diiodo-bis(2,2'bipyridylamine)Copper(II)Iodide Perchlorate", J. Chem. Soc., Dalton 580 (1973).
  71. Gress, M. E. and Jacobson, R. A., "1,2,3,4,10,10-Hexachloro-6,7-Exo- Epoxy-1,4,4a,5,6,7,8,8a-Octahydro-Endo-Exo-1,4:5,8-Dimethanonaphthalene (Dieldrin), C12H8C16O", Cryst. Struct. Comm. 2, 485 (1973).
  72. Lawton, S. L., McAfee, E. R., Benson, J. E., and Jacobson, R. A., "Crystal Structure of Quinolinium Hexabromoantimonate(V) Tribromide, (C9H7NH)2SbVBr9", Inorg. Chem. 12, 2939 (1973).
  73. Gress, M. E. and Jacobson, R. A., "X-Ray and White Radiation Neutron Diffraction Studies of Optically Active Postassium Antimony Tartrate, K2Sb2(d-C4H2O6)2·3H2O (Tartar Emetic)", Inorg. Chim. Acta 8, 209 (1974).
  74. Wismer, R. K. and Jacobson, R. A., "The Crystal and Molecular Structure of trans-cyano Triethylenetetramine Cobalt(III) Perchlorate", Inorg. Chim. Acta 7, 477 (1973).
  75. Rohrbaugh, W. J. and Jacobson, R. A., "The Crystal and Molecular Structure of the Decacoordiante Complex Tris(bicarbonato)- Tetraquoholmium(III) Dihydrate, Ho(H2O)4(HCO3)3·2H2O", Inorg. Chem. 13, 2535 (1974).
  76. Wismer, R. K. and Jacobson, R. A., "Crystal Structure of Potassium Pentachloroantimonate(III)", Inorg. Chem. 13, 1678 (1974).
  77. Hubbard, C. R., Quicksall, C. O., and Jacobson, R. A., "A Neutron Diffraction Study of the Holmium Ethylsulfate Enneahydrate by the White Radiation Method", Acta Cryst. B30, 2613 (1974).
  78. Gorres, B. T., McAfee, E. R., and Jacobson, R. A., "The Crystal and Molecular Structure of ß-Picoline-N-Oxide Fumaric Acid Adduct", Acta Cryst. B31, 158 (1975).
  79. Rodgers, J. and Jacobson, R. A., "An X-Ray Investigation of DL- (ethylvalinate-N,N-diacetato)diaquo Copper(II)", Inorganica Chimica Acta 13, 163 (1975).
  80. Brassfield, H. A., Jacobson, R. A., and Verkade, J. G., "Molecular Structure of the Carcinostat Isophosphamide", Amer. Chem. Soc. 97, 4143 (1975).
  81. Jensen, W. P., Jacobson, R. A., and Benson, J. E., "Dodecamethyl Cyclohexagermaine, C12H36Ge6", Cryst. Struct. Comm. 4, 299 (1975).
  82. Baughman, R. G. and Jacobson, R. A., "The Crystal and Molecular Structure of Organophosphorus Insecticides. I. Ronnel", Agricultural and Food Chemistry, 23(4), 811 (1975).
  83. Warner, P., Lu, S.-L., Myers, E., DeHaven, P. W., and Jacobson, R. A., "Propellanes. VII. Bridgehead Olefins Via Acetolysis", Tetrahedron Letters 50, 4449 (1975).
  84. Martin, Jr., D. S., Bonte, J. L., Rush, R. M., and Jacobson, R. A., "Potassium Tetrabromopalladate(II)", Acta Cryst. B31, 10 (1975).
  85. Gifkins, M. R. and Jacobson, R. A., "Crystal and Molecular Structure of Organophosphorus Insecticides. II. Coroxon", J. Agr. and Food Chem. 24(2), 232 (1976).
  86. Jacobson, R. A., "A Single-Crystal Automatic Indexing Procedure", J. Appl. Cryst. 9, 115 (1976).
  87. DeHaven, P. W. and Jacobson, R. A., "Pyridinium Tetrabromoantimonate(III), C5H5NH SbIIIBr4", Crystal Struct. Comm. 5, 31 (1976).
  88. Stadel, P., Jensen, Wm., Worman, J. and Jacobson, R. A., "The Crystal Structure of N,N'-Bis-p-Bromophenyl-2,2,4,4-tetramethy1cyclo-butane-1,3-di-imine", J. Chem. Society (Perkin 2), 5, 536 (1976).
  89. Miller, J. H., Powell, J. E., Jacobson, R. A., and Kulprathipanja, S., "The Crystal and Molecular Structure of Diaquobis (2,3-dihydroxy-2-methylpropanoato)Copper(II)", Inorg. Chim. Acta 18, 25 (1976).
  90. Fuller, C. C. and Jacobson, R. A., "Tris(Nitrato)Tetra-aquopraseodymium(III) Dihydrate, Pr(NO3)3(H2O)4·2H2O", Cryst. Struct. Comm. 5, 349 (1976).
  91. Rohrbaugh, W. J., Meyers, E. K., and Jacobson, R. A., "The Crystal and Molecular Structure of Organophosphorus Insecticides. 3. Azinphos-Methyl", J. Agr. and Food Chem. 24(4), 713 (1976).
  92. Takusagawa, Fusao and Jacobson, R. A., "Crystal Structure Studies of Tetragonal Sodium Tungsten Bronzes, NaxWO3. I. Na0.33WO3 and Na0.48WO3", J. Solid State Chem. 18, 163 (1976).
  93. Baughman, R. G. and Jacobson, R. A., "The Crystal and Molecular Structure of Organophosphorus Insecticides, IV. Bromophos", J. Agr. Food Chem. 24, 1036 (1976).
  94. Woodard, S. S., Jacobson, R. A., and Angelici, R. J., "Structure of trans-W(CO)4(CNC6H11)(CS) and a Correlation of O(CS) Frequencies with vC-S Bond Distances in Metal Thiocarbonyl Complexes", J. Organometallic Chem. 117, C75 (1976).
  95. Takusagawa, Fusao, Jacobson, R. A., Trahanovsky, W. S., and Robbins, D., "Phenyltropylium Fluoroborate-Triphenylmethyl Fluoride", Cryst. Struct. Comm. 5, 753 (1976).
  96. Peters, C., Jensen, Wm. P., Worman, J. J., Jacobson, R. A., and Nelson, D. A., "The Crystal Structure of 3,7-Dihydroxy-1,5-Bis(P-Bromophenyl) Octahydro-1,5-Diazocine Ethanol Solvate, C18H2Br2N2O2·C2H6O", Cryst. Struct. Comm. 5, 905 (1976).
  97. Peters, C. Y., Jensen, Wm. P., Worman, J. J., Jacobson, R. A., and Nelson, D. A., "The Configuration and Solid State Conformation of 3,7-Dihydroxy-1,5-bis(p- bromophenyl)octahydro-1,5-diazocine", J. Heterocyclic Chem. 14, 769 (1977).
  98. Baughman, R. G. and Jacobson, R. A., "Crystal and Molecular Structure of Organophosphorus Insecticides. 5. Fospirate", J. Agr. Food Chem. 25(3), 582 (1977).
  99. Helland, B. J., Quick, M. H., Jacobson, R. A., and Angelici, R. J., "Crystal and Molecular Structure of an Organic Thiocyanate Complex: (CH3SCN)Cr(CO)5" J. Organometallic Chem. 132, 95 (1977).
  100. Rohrbaugh, W. J. and Jacobson, R. A., "Crystal and Molecular Structure of Organophosphorus Insecticides. 6. Amidithion", J. Agr. Food Chem. 25(3), 588 (1977).
  101. Takusagawa, Fusao and Jacobson, R. A., "The Crystal and Molecular Structure of Carbamate Insecticides. I. Mesurol", J. Agr. Food Chem. 25(2), 329 (1977).
  102. Takusagawa, Fusao and Jacobson, R. A., "Crystal and Molecular Structure of Carbamate Insecticides. 2. Aldicarb", J. Agr. Food Chem. 25(2), 33 (1977).
  103. Takusagawa, Fusao and Jacobson, R. A., "The Crystal and Molecular Structure of Carbamate Insecticides. 3. Methomyl", J. Agr. Food Chem. 25(3), 577 (1977).
  104. Warner, Philip, M., Lu, Shih-Lai, Myers, Elaine, DeHaven, Patrick, W., and Jacobson, R. A., "Propellanes. 17. Bridgehead Olefins via Solvolysis of 10,10- Dibromo[4.3.1]propellanes", J.A.C.S. 99, 5102 (1977).
  105. Karcher, Barbara A. and Jacobson, R. A., "Crystal and Molecular Structure of Cr(CO)5(SCMe2), A Thioketone Complex", J. Organometallic Chem. 132, 387 (1977).
  106. Rohrbaugh, W. J. and Jacobson, R. A., "Tris(ethylenediamine)-cobalt(III) Tetrakis(isotiocyanato)cobaltate(II) Nitrate", Acta Cryst. B33, 3254 (1977).
  107. Templeton, J. L., Jacobson, R. A., and McCarley, R. E., "Synthesis and Structure of Bis(tetrapropylammonium)tri-μ-·-bromohexabromoditungstate(2-). A Novel Odd-Electron Dimeric Anion Showing Evidence of Jahn Teller Distortion", Inorg. Chem 16, 3320 (1977).
  108. Voss, K. E., Angelici, R. J., and Jacobson, R. A., "Crystal and Molecular Structure of υ[-N-(o-hydroxybenzyl](L-alaninato)cobalt(III) Dihydrate", Inorg. Chem. 17, 1922 (1978).
  109. Takusagawa, Fusao and Jacobson, R. A., "The Crystal and Molecular Structure of -Maltose", Acta Cryst. B34, 213 (1978).
  110. Ho, Dominic, Riley, Walter C., and Jacobson, R. A., "The Crystal and Molecular Structure of Cs3Sb2I9", Cryst. Struct. Comm. 7, 111 (1978).
  111. MacDougall, J. Jeffrey, Nelson, John H., Babich, Michael W., Fuller, Charles, C., and Jacobson, R. A., "Coordination Behavior of Thiocyanate in the Complex [CH3P(C6H5)2]2M(CNS)2; M-Ni,Pd,Pt", Inorg. Chim. Acta 27, 201 (1978).
  112. Rohrbaugh, W. J. and Jacobson, R. A., "The Crystal and Molecular Structure of Organophosphorus Insecticides. 9. Stirofos", J. Agr. Food Chem. 26, 1120 (1978).
  113. Baughman, R. G., Jorgensen, S. K., and Jacobson, R. A., "The Crystal and Molecular Structure of Organophosphorus Insecticides. 10. Chlorpyrifos", J. Agr. Food Chem. 26, 576 (1978).
  114. Baughman, R. G. and Jacobson, R. A., "The Crystal and Molecular Structure of Organophosphorus Insecticides. 8. Ronnel Oxon", J. Agr. Food Chem. 26, 403 (1978).
  115. Baughman, R. G., Virant, M. S., and Jacobson, R. A., "The Crystal and Molecular Structure of Herbicides. I. Pyrazon", J. Agr. Food Chem. 26, 511 (1978).
  116. Wagner, R. E., Jacobson, R. A., Angelici, R. J., and Quick, M. H., "Synthesis of Thiocarbonyl-Bridged (ν5-C5H5)2Fe2(CO)3(CS) and Crystal Structure of an S-Alkylated Derivative", J. Organometal. Chem. 148, C35 (1978).
  117. Baughman, R. G., Eckey, D. A., and Jacobson, R. A., "The Crystal and Molecular Structure of Organophosphorus Insecticides. 7. Crufomate", J. Agr. Food Chem. 26, 398 (1978).
  118. Stensvand, S., Helland, B., Babich, M., Jacobson, R., and McCarley, R., "The Molybdenum Iodide Cluster Anion Mo4I112-. A New Cluster Type Structurally Related to the Mo6I84+ Octahedral Cluster", J. Am. Chem. Soc. 100, 6257 (1978).
  119. Fuller, C. C., Molzahn, D. K., and Jacobson, R. A., "Crystal and Molecular Structure of the Decacoordinate Compound ((Hydroxyethyl)ethyl- enediaminetriacetato)diaquolanthanum(III) Trihydrate", Inorg. Chem. 17, 2138 (1978).
  120. Ma, M. S., Angelici, R. J., Powell, D., and Jacobson, R. A., "Unusual Coordination of the α-Dioxime Ligand in Bis(camphorquinone dioximato(nickel(II)", J. Am. Chem. Soc. 100, 7068 (1978).
  121. Beckman, D. E. and Jacobson, R. A., "Crystal and Molecular Structure of (C5H5)2Fe2(CO)3CS", J. Organometal. Chem. 179, 187 (1979).
  122. Beckman, D. E. and Jacobson, R. A., "The Crystal and Molecular Structure of Organophosphorus Insecticides. 12. Dowco 214", J. Agr. Food Chem. 27(4), 712 (1979).
  123. Jacobson, R. A. and Beckman, D. E., "A Modified Patterson Superposition Technique Using Multiple Vectors", Acta Cryst. A35, 339 (1979).
  124. Ebner, S. R., Jacobson, R. A., and Angelici, R. J., "Preparation, Structure, and Spectral Characterization of Bis[D-ß-(2-pyridyl)-α- alaninato]cobalt(III), CO(D-Pyala)2<+&", Inorg. Chem. 18, 765 (1979).
  125. DeHaven, P. W. and Jacobson, R. A., "Profile Refinement of Multiple Wavelength Neutron Powder Data", J. Applied Cryst. 12, 601 (1979).
  126. Fuller, C.C., Murphy, P. D., and Jacobson, R. A., "Hydroxyethylethylenediaminetriacetodiaquocerium(III) Trihydrate Dimer, {Ce[(O2CCH22NCH2CH2N(CH2CH2OH)(CH2CO2)(H2O)]·3H2O}2", Cryst. Struct. Comm. 8, 9 (1979).
  127. White, D. W., Karcher, B. A., Jacobson, R. A., and Verkade, J. G., "A Tris(dialkylamino)phosphine with Pyramidal Nitrogens", J. Am. Chem. Soc. 101, 4921 (1979).
  128. Krishnanachari, N. and Jacobson, R. A., "Diisopropy1-2,3,4,5-Tetraphenyl- cyclopenta-1,4-Dienyl Phosphate, C35H35O4P", Cryst. Struct. Comm. 8, 873 (1979).
  129. Greaves, W. W., Angelici, R. J., Helland, B. J., Klima, R. J., and Jacobson, R. A., "Synthesis and Structure of ( ν-C5H5)-W(PPh3)(CO)(CS-Ph): Transformation of a Thicarbonyl Ligand into a Carbyne Ligand", J. Am. Chem. Soc 101, 7618 (1979).
  130. Ebner, S. R., Helland, B. J., Jacobson, R. A., and Angelici, R. J., "Preparation, Structure, and Spectral Characterization of Bis[D-ß-(2-α pyridyl)--alaninato]nickel(II), Ni(D-Pyala)2", Inorg. Chem. 19, 175 (1980).
  131. Lapp, R. L. and Jacobson, R. A., "The Crystal and Molecular Structure of Organophosphorus Insecticides. 13. Isopropyl-O-methyl-0-(3,5,6-Trichloro-2-pyridyl) Phosphoramidothioate and Dimethoate", J. Agr. Food Chem. 28, 755 (1980).
  132. Matsui, M., Watanabe, T., Lapp, R. L., and Jacobson, R. A., "The Crystal Structures of ß-Ca(HCOO)2 and d-Ca(HCOO)2, and the Tetragonal Mixed Crystals Ca(HCOO)2-Sr(HCOO)2", Acta Cryst. B36, 1081 (1980).
  133. Lapp, R. L. and Jacobson, R. A., "O-Methyl-O-(4-Bromo-2,5 Dichlorophenyl)-Phenylphosphonothioate, Cl2BrPSO2C13H10", Cryst. Struct. Comm. 9, 65 (1980).
  134. Ma, M. S., Angelici, R. J., Powell, D., and Jacobson, R. A., "Coordination Chemistry of Bis(d-camphorquinonedioximato)Ni(II) and Pd(II). Reactions and Structural Studies of Some M3Ag3 Cluster Complexes of Camphorquinone-Dioxime", Inorg. Chem. 19, 3121 (1980).
  135. Muller, F. A. and Jacobson, R. A., "Tetrahydro-3,4-Furandione, CD4H4O3", Cryst. Struct. Comm. 9, 325 (1980).
  136. Meiske, L. A., Jacobson, R. A., and Angelici, R. J., "Synthesis, Spectral Characterization and Molecular Structure of [N-(2-pyridylmethyl)-L-aspartato]-[L- phenylalaninato]cobalt(III) Trihydrate, [Co(PLASP)(L-Phe)]·3H2O", Inorg. Chem. 19, 2028 (1980).
  137. Allahyari, R., Hollingshaus, J. G., Lapp, R. L., Timm, E., Jacobson, R. A., and Fukuto, T. R., "Resolution, Absolute Configuration, Acute and Delayed Neurotoxicity of the Chiral Isomers of O-Aryl O-Methyl Phenylphosphonothioate Analogs Related to Leptophos", J. Agr. Food Chem. 28, 594 (1980).
  138. Warner, P., Chang, S., Powell, D. R., Grewe, T. E., and Jacobson, R. A., "On the Dimerizaton of Bridgehead Olefins Formed From Tricyclic Cyclopropylidenes", J. Am. Chem. Soc. 102, 5125 (1980).
  139. Shelton, R. N., Karcher, B. A., Powell, D. R., Ku, H. C., and Jacobson, R. A., "Crystal Structure of LuRuB2", Mat. Res. Bull. 15, 1445 (1980).
  140. Gifkins, M. R. and Jacobson, R. A., "O-Ethyl-O-(4-Nitrophenyl) Benzene Phosphonothioate (EPN)", Cryst. Struct. Comm. 9, 571 (1980).
  141. Baughman, R. G., Hembre, R. I., Helland, B. J., and Jacobson, R. A., "3-(p-Chlorophenyl)-1,1-Dimethylurea(Monuron), C9H11ClN2O", Cryst. Struct. Comm. 9, 749 (1980).
  142. Gifkins, M. R. and Jacobson, R. A., "N'-(4-Chloro-o-tolyl)-N,N-Dimethylformamidine (Chlordimeform), C10H13ClN2", Cryst. Struct. Comm. 9, 959 (1980).
  143. Baughman, R. G., Sams, D. D., Helland, B. J., and Jacobson, R. A., "3-(3,4-Dichlorophenyl)-1,1-Dimethylurea(Diuron), C9H10Cl2N2O", Cryst. Struct. Comm. 9, 885 (1980).
  144. Powell, D. R. and Jacobson, R. A., "The Crystal and Molecular Structure of cis-Dichlorobis(Methyldiphenylphosphinite) Palladium(II), PdCl2[P(OMe)Ph2]2". Cryst. Struct. Comm. 9, 1023 (1980).
  145. Walsh, J. J., Metzler, D. E., Powell, D., and Jacobson, R. A., "2- Hydroxymethylaspartic Acid: Synthesis, Crystal Structure and Reaction with a Transaminase", J. Am. Chem. Soc. 102, 7136 (1980).
  146. Warner, Philip, Chen, Bing-Lin, Bronski, Catherine A., Karcher, Barbara A., and Jacobson, R. A., "Synthesis of Some [n.1.3.1]- and [n.1.2.1]Paddlanes", Tetrahedron Letters 22, 375 (1981).
  147. Pickering, R. A., Jacobson, R. A., and Angelici, R. J., "Reactions of the Dithiocarbene Complex W(CO)5[C(SCH3)2] with Phosphines. Crystal Structure of a Phosphorane Product W(CO)5[(CH3S)2C=PPh2(CH3)]", J. Am. Chem. Soc. 103, 817 (1981).
  148. Fuller, C. C. and Jacobson, R. A., "The Crystal and Molecular Structure of Bis(O-tricyanoethyleneoate)bis(2,2',N,N'-bispyridylamine)copper(II)", Inorg. Chim. Act 48, 191 (1981).
  149. Hariharan, A. V., Powell, D. R., Jacobson, R. A., and Franzen, H. F., "The Crystal Structure of Lu3S4: A New Population Wave Structure", J. Solid State Chemistry 36, 148 (1981).
  150. Jensen, W. P. and Jacobson, R. A., "The Structure of Chlorobis- (2,2',N,N'bipyridyl)copper(II)(1,1,2,3,3-pentacyanopropenide)", Inorg. Chim. Acta 50, 189 (1981).
  151. Meiske, L. A., Jacobson, R. A., and Angelici, R. J., "Synthesis and Spectral Characterization of fac- and mer-[N-(Carboxymethyl)-L-ß-(2-pyridyl)-α-alaninato](D-threoninato)cobalt(III), [Co(N-Cm-L-Pyala)(D- Thr)], and the Molecular Structure of the mer Isomer", Inorg. Chem. 20, 1794 (1981).
  152. Jacobson, R. A., Karcher, B. A., Montag, R. A., Socol, S. M., Vande Griend, L. J., and Verkade, J. G., "Crystal and Molecular Structure of Bis(cis-2-Methoxy-4,6-Dimethyl-1,3,2- Dioxaphosphorinane)Tetra-Carbonyl-Molybdenum(O) - A Complex Containing a Thermodynamically Unstable Ligand Isomer", Phosphorus and Sulfur 11, 27 (1981).
  153. Jensen, W. P. and Jacobson, R. A., "The Structure of Bis-2,2',N,N' Bipyridylamine Copper(II) Chloride Tetra Hydrate", Inorg. Chim. Acta 49, 199 (1981).
  154. Powell, D. R. and Jacobson, R. A., "The Crystal Structure of 3-R Nb1.06S2", J. Solid State Chem. 37, 140 (1981).
  155. Klima, R. and Jacobson, R. A., "Dimethyl(2,2,2-Trichloro-1-Hydroxyethyl)-Phosphonate (Trichlorofon), C4H7Cl3O4P", Cryst. Struct. Comm. 10, 901 (1981).
  156. Jacobson, R. A. and Jensen, W. P., "The Crystal and Molecular Structure of Bis-aqua-2,2',N,N'bipyridylamine Fluoro Copper(+1) Fluoride Trihydrate", Inorganica Chim. Acta 52, 205 (1981).
  157. Jacobson, R. A. and Jensen, W. P., "The Crystal and Molecular Structure of 2,2',N,N'-bipyridyl Chloro Tricyanoethenolate Copper(0)", Inorganica Chim. Acta 52, 219 (1981).
  158. Baughman, R. S., Virant, M. S., and Jacobson, R. A., "Crystal and Molecular Structure of Herbicides. 4. Bromoxynil", J. Agr. Food Chem. 29, 989 (1981).
  159. Riley, W. C. and Jacobson, R. A., "1-(4-chloropheny1)-3-(2-6- Difluorobenzoyl)Urea(Difluorbenzuron)", Cryst. Struct. Comm. 10, 1341 (1981).
  160. Moss, L. E. and Jacobson, R. A., "N-(Trichloromethylthio)-3a,4,7,7a-Tetra-hydrophthalimide (Captan), C9H8NO2SCl3", Cryst. Struct. Comm. 10, 1545 (1981).
  161. McCormick, F. B., Angelici, R. J., Pickering, R. A., Wagner, R. E., and Jacobson, R. A., "Preparation of (ν5-Cyclopentadienyl)dicarbonyl-[tri(organothio)methyl]iron Complexes and the Structure of Cp(CO)2Fe[C(SCH3)2]", Inorg. Chem. 20, 4108 (1981).
  162. Warner, P., Chang, S.-C., Powell, D. R., and Jacobson, R. A., "Synthesis and Molecular Structure of a Tetra-t-Butylethylene Derivative Obtained From a Propellanic Carbenoid", Tet. Letters 22, 533 (1981).
  163. Bendiksen, B., Riley, W. C., Babich, M. W., Nelson, J. H., and Jacobson, R. A., "The Crystal and Molecular Structures of [C6H5CH2)3P]2PdX2; X = CN, N3", Inorg. Chim. Acta 57, 29 (1982).
  164. Yu, Y. S., Jacobson, R. A., and Angelici, R. J., "Synthesis, Structure, and Reactions of 19-Electron (ν5-C5H5)W(NO)2(PR3) Radicals", Inorg. Chem. 21, 3106 (1982).
  165. Burow, M. D., Karcher, B. A., and Jacobson, R. A., "2-Chloro-N-(2',6'- Diethylphenyl)-N-(Methoxy-Methyl)Acetamide (Alachlor), C14H20ClNO2", Cryst. Struct. Comm. 11, 747 (1982).
  166. Abicht, Von H.-P, Baumeister, U., Hartung, H., und Issleib, K., Halle (Saale), Sektion Chemie der Martin-Luther-Universitat, Jacobson, R. A., Richardson, J. W., Socol, S. M., and Verkade, J. G., "Zur Metallierung von Benzylphosphinen II", Z. Anorg. Allg. Chem. 494, 55 (1982).
  167. Carpenter, L. E., Powell, D., Jacobson, R. A. and Verkade, J. G., "Crystal and Molecular Structure of bis(2-ß-Chloroethylamino)-4,6- dimethyl-1,2,3-oxazaphosphorinane: An Analogue of Cyclophosphamide", Phosphorus Sulfur 12, 287 (1982).
  168. Wilkes, L. M., Nelson, J. H., Mitchener, J. P., Babich, M. W., Riley, W. C., Helland, B. J., Jacobson, R. A., Cheng, M. Y., Seff, K., "Ruthenium(II) Complexes of Benzyl Phosphines", Inorg. Chem. 21, 1376 (1982).
  169. Jacobson, R. A., "Robert E. Rundle", in Crystallography in North America edited by Dan McLachlan, Jr. and Jenny P. Glusker, American Crystallographic Association, p 120 (1983).
  170. Jacobson, R. A., "The Fast Fourier Transform in Crystallography", in Crystallography in North America edited by Dan McLachlan, Jr. and Jenny P. Glusker, American Crystallographic Association, p 233 (1983).
  171. Neckers, D. C., Wagenaar, F. L., Hauenstein, D. and Jacobson, R. A., "Photochemical Cycloadditions of 2,3-Dihalobenzo(b)thiophenes" Stereochemical and Mechanistic Results", J. Organic Chem. 48, 1725 (1983).
  172. Muller, R., Shelton, R. N., Richardson, Jr., J. W., and Jacobson, R. A., "Superconductivity and Crystal Structure of a New Class of Ternary Transition Metal Phosphides TT'P (TZr,Nb,Ta and T'Ru,Rh)", J. Less-Common Metals 92, 177 (1983).
  173. Shelton, R. N., Horng, H. E., Bevolo, A. J., Richardson, Jr., J. W., Jacobson, R. A., Bader, S. D., and Hamaker, H. C., "Charge Transfer and Transition-Metal Cluster: Boron Bonding in the bct Superconducting Y(Rh1- xRux)4B4 System", Physical Review B, 27(11) (1983).
  174. Lesch, D. A., Richardson, Jr., J. W., Jacobson, R. A. and Angelici, R. J., "Reactions of the -Thiophene Ligand in (ν-C4H5S)Mn(CO)3+. Mechanistic Possibilities for Catalytic Hydrodesulfurization", J. Am. Chem. Soc. 106, 2901 (1984).
  175. Kim, Heesook P., Kim, Sangsoo, Jacobson, Robert A. and Angelici, Robert J., "Synthesis of an ν2-CH(SMe) Carbene Ligand by Protonation of the Carbyne in [HB(pz)3](CO)2W(C-SME). A Possible Model Step in CO Hydrogenation", Organometallics 3, 1124 (1984).
  176. Amenson, J., Benson, J., Demirel, T. and Jacobson, R., "Quantitative Analysis: A Comparative Study Using Mo and Cu Radiation on Coal Related Minerals and Fly Ash", Advances in X-Ray Analysis 27, 349 (1984).
  177. Lindsay, Alan J., Kim, Sangsoo, Jacobson, Robert A. and Angelici, Robert J., "Synthesis from Diamines of Mono- and Dinuclear Cyclopentadienyliron Dicarbonyl Carbamoyl Compounds. Crystal and Molecular Structure of (μ-CONH(CH2)2NHCO)[CpFe(CO)2]2", Organometallics 3, 1523 (1984).
  178. Plummer, Daniel T., Karcher, Barbara A., Jacobson, Robert A. and Angelici, Robert J., "Synthesis of Chelating Trimethylsiloxy Diisonitrile Ligands and Their Rhodium(I) Complexes. Crystal and Molecular Structure of [Rhl(t-BudiNC)2]BPh4·5CH3CN (DiNC = chelating bidentate isonitrile ligand)", J. Organometallic Chem. 260, 347 (1984).
  179. Lacelle, S., Stevenson, W. C., Kurtz, Jr., D. M., Richardson, Jr., J. W., and Jacobson, R. A., "Crystal and Molecular Structure of [Cd10(SCH2CH2OH)16](Cl04)4·8H2O. Correlations with 113Cd NMR Spectra of the Solid and Implications for Cadmium-Thiolate Ligation in Proteins", Inorg. Chem. 23, 930 (1984).
  180. Schiff, D. E., Richardson, Jr., J. W., Jacobson, R. A., Cowley, A. H., Lasch, J. and Verkade, J. G., "Stereoelectronic Effects of Cyclization in Aminophosphine Systems: Structural, PES, and NMR Study of Me2NP(OCH2)2CMe2 and CH2(CH2CH2)2NP(OCH2)2CMe2", Inorg. Chem. 23, 3373 (1984).
  181. Socol, S. M., Jacobson, R. A. and Verkade, J. G., "Ligation of Phosphorus Ligands to Silver(I). 1. Coordination of One to Four P(NR2)3 Ligands and the Structure of a Nonlinear Two-Coordinate Complex", Inorg. Chem. 23, 88 (1984).
  182. Schroeder, N. C., Richardson, Jr., J. W., Wang, S.-L., Jacobson, R. A. and Angelici, R. J., "Reaction of Co(CO)4- with a Bridging Carbyne Complex, [Cp2Fe2(CO)2(μ-CO)(μ-CSMe)]PF6. Crystal and Molecular Structures of Cp2Fe2Co(CO)3(μ3-CSMe) and Cp2Fe2Co(CO)2(PPh3)(μ-CO)2(μ3- CSMe)", Organometallics 4, 1226 (1985).
  183. Koetzle, T. F., Schoenborn, B. P., Arndt, U. W., Basie, J. K., Jacobson, R. A., Lehmann, M. S., Mason, S. A. and Schultz, A., J., "Crystallography (single crystal and protein)", in "Scientific Opportunities for Neutron Diffraction". G. H. Lander, V. J. Emery (eds). Nucl. Inst. and Meth. B12, 537 (1985).
  184. Kim, H. P., Kim S., Jacobson, R. A. and Angelici, R. J., "Syntheses and Structures of [HB(pz)3](CO)2(CS)W-Au(PR3). First Examples of a Semibridging CS Ligand:, J. Am. Chem. Soc. 108, 5154 (1986).
  185. Blau, R. J., Espenson, J. H., Kim, S. and Jacobson, R. A., "Characterization, Structure, and Conformations of a Dinuclear Platinum(I) Complex with Mixed Halide-Phosphine Ligands Trans to the Metal-Metal Bond", Inorg. Chem. 5, 757 (1986).
  186. Chen, Y.-S., Wang, S.-L., Jacobson, R. A. and Angelici, R. J., "Substitution and Fragmentation Reactions of Br2Os3(CO)12 with Phosphines. Structure of Br2Os3(CO)10[P(OMe)3]2", Inorg. Chem. 25, 1118 (1986).
  187. Jacobson, R. A. and Jensen,W. P., "Anhydrous Bis-2,2',N,N'-Bipyridylamine-chloro-Copper(II) Chloride", Inorg. Chim. Acta 114, L9 (1986).
  188. Jacobson, R. A., "An Orientation Matrix Approach to Laue Indexing", J. Appl. Crystal. 19, 283 (1986).
  189. Benson, J. E., Struble, R. E. and Jacobson, R. A., "A Diffraction-Based Pyrite Monitor", Coal Prep. 3, 213 (1987).
  190. Richardson, Jr., J. W. and Jacobson, R. A., "Computer-Aided Analysis of Multi-Solution Patterson Superpositions", Symposium on the Patterson Function, J. P. Glusker Publ., Ed. J. P. Glusker, B. K. Patterson, and M. Rossi, Oxford University Press, Oxford, Engl., pp 311-317 (1987).
  191. Larock, R. C., Burns, L. D., Varaprath, S., Russell, C. E., Richardson, Jr., J. W., Janakiraman, M. N. and Jacobson, R. A., "Mercury in Organic Chemistry. 34.1 Synthesis of Vinylmercurials Via Mercuration of Propargylic Amines", Organometallics 5, 1780 (1987).
  192. Wang, S.-L., Richardson, Jr., J. W., Briggs, S. J., Jacobson, R. A. and Jensen, Wm. P., "Stabilization of a Hydrated Ketone by Metal Complexation. The Crystal and Molecular Structures of Bis-2,2',N,N'-Bipyridyl Ketone-Hydrate Nickel(II) Sulfate, Copper(II) Chloride and Copper(II) Nitrate", Inorg. Chim. Acta 111, 67 (1986).
  193. Lii, K.-H., McCarley, R. E., Kim, S. and Jacobson, R. A., "Synthesis and Structure of Ternary Molybdenum Oxides MMo8O10 (M = Li or Zn) Having Orthogonal Nonintersecting Octahedral Cluster Chains", Solid State Chem. 64, 347 (1986).
  194. Kim, H. P., Kim, S., Jacobson, R. A. and Angelici, R. J., "Reactions of Thiocarbyne [HB(pz)3](CO)2W( CSMe) and Thiocarbene [HB(pz)3](CO)2W[ν2- CH(SMe)]+ Complexes with Phosphines", Organometallics 5, 2481 (1986).
  195. Moss, L. E., Karcher, B. A., Richardson, Jr., J. W. and Jacobson, R. A., "The Crystal and Molecular Structure of SO3N2C10H11: 3-Isopropyl-1,1,3- Benzothiazian-4-one-2,2-Dioxide (BENTAZON)", Acta Cryst. C42, 1785 (1986).
  196. Angus, R. O., Jr., Janakiraman, M. N., Jacobson, R. A. and Johnson, R. P., "Small-Ring Cyclic Cumulenes: Synthesis and X-Ray Crystal Structure of Bis(Triphenylphosphine)chloro(ν2 -1,2,3-cyclononatriene)rhodium", Organometallics 6, 1909 (1987).
  197. Bush, R. C., Jacobson, R. A. and Angelici, R. J., "Synthesis and Structure of [l-5-ν-6-exo-Re(CO)5-C7H8]Mn(CO)3. The First Example of Metal Carbonyl Anion Addition to a Coordinated Cyclic π-Hydrocarbon", J. Organometal. Chem. 323, C25 (1987).
  198. Richardson, Jr., R. J., Angelici, R. A. and Jacobson, R. A., "Structure of [ν-C5H5Fe(CO)2(CS)]PF6, A Comparison of M-CS and M-CO Bonding", Inorg. Chem. 26, 452 (1987).
  199. Miessler, G. L., Kim, S., Jacobson, R. A. and Angelici, R. J., "Syntheses, Reactions, and Structures of Dioxycarbene Complexes of Rhenium", Inorg. Chem. 26, 1690 (1987).
  200. Anglin, R. J., Kurtz, Jr., D. M., Kim, S. and Jacobson, R. A., "Synthesis and Structure of the Linear Tetranuclear Cluster [(MoO2S2)2Fe2S2]4-: Implications for Aqueous Mo-Fe-S Chemistry", Inorg. Chem. 26, 1470 (1987).
  201. Larock, R. C., Song, H., Kim, S. and Jacobson, R. A., "Synthesis, Stereochemistry, Mechanism of Formation, and X-ray Crystal Structures of Optically Active π-Allylpalladium Compounds Formed Via Palladium-Promoted Ring Opening of Bicyclic Alkenes", Chem. Communications. 834 (1987).
  202. Hurng, W.-M., Corbett, J. D., Wang, S.-L. and Jacobson, R. A., "A Zintl Phase with a Layered Network Structure KSi3As3", Inorg. Chem. 26, 2392 (1987).
  203. Jacobson, R. A. and Swenson, R. W., "Computer-Aided Degree Planning", NACADA Proceedings of the Ninth National Conference on Academic Advising, V. F. Dailey, Editor, pp. 48-9 (1986).
  204. Jacobson, R. A., Book Review of Ronald N. Bracewell, "The Hartley Transform", Mathematics of Computation, Vol. 48, 178, pp. 449-858, (1987).
  205. Huckett, S. C., Miller, L. L., Jacobson, R. A. and Angelici, R. J., "Ru, Rh, and Ir Complexes of π-Bound Thiophene and Benzo[b]thiophenes: Models for Thiophene Binding to HDS Catalysts", Organometallics 7, 686 (1988).
  206. Yeo, I.-H., Kim, S., Jacobson, R. A. and Johnson, D. C., "Electrocatalysis of Anodic Oxygen Transfer Reaction: Comparison of Structural Data with Electrocatalytic Phenomena for Bismuth-Doped Lead Dioxide", J. Electrochemical Soc. 136, 1395 (1989).
  207. Krassowski, D. E., Nelson, J. W., Brower, K. R., Hauenstein, D. and Jacobson, R. A., "Kinetic and Thermodynamic Stabilities of the Geometric Isomers of (R3P)2Ru(CO)2Cl2 and (R3P)3Ru(CO)Cl2 Complexes", Inorg. Chem. 27, 4294 (1988).
  208. Miller, L. L. and Jacobson, R. A., "A Self-Consistent Semi-Empirical Absorption Correction Technique", Computers and Chem. 13, 1, 1-3 (1989).
  209. Wroblewski, A. E., Applequist, J., Takaya, A., Honzatko, R., Kim, S.-S., Jacobson, R. A., Reitsma, B. H., Yeung, E. S. and Verkade, J. G., "An Experimental and Theoretical Study of the Structures and Optical Rotations of Chiral Bicyclic Ortho Esters", J. Am. Chem. Soc. 110, 4144 (1988).
  210. Klimyenko, A. V., Seuntjens, J., Miller, L. L., Beaudry, B. J., Jacobson, R. A. and Gschneidner, Jr., K. A., "Structure of LaNi2.286 and the La-Ni System from LaNi1.75 to LaNi2.50", J. Less-Common Metals 144, 133 (1988).
  211. Kraus, G. A., Thurston, J., Thomas, P. J., Jacobson, R. A. and Su, Yingzhong, "2-Benzoyloxynitroethylene as a Cis-2-Aminoethenol Equivalent", Tet. Letters 29, 1879 (1988).
  212. Schwarz, W. H. E., Mensching, L., Ruedenberg, K., Jacobson, R. A. and Miller, L. L., "X-Ray Diffraction, Electron Densities and Chemical Bonding", Portgal. Phys. 19, 185 (1988).
  213. Spencer, J. T., Spencer, J. A., Jacobson, R. A. and Verkade, J. G., "Spectroscopic and Structural Effects of Electronegative Phosphorus Bridges in a New Series of Phosphido Complexes: Cis and Trans-[ν5-C5H5)Fe(CO)4(μ2-L)]2 and [(ν4-C5H6)Fe(CO)(μ2-L)Fe(CO)3]", New J. Chem. 13, 275 (1989).
  214. Lipscomb, Wm. N. and Jacobson, R. A., "X-Ray Crystal Structure Analysis", Book Chapter in Physical Methods of Chemistry, Second Edition, Volume V, Determination of Structural Features of Crystalline and Amorphous Solids, Ed., B. W. Rossiter and J. F. Hamilton, Wiley & Sons, Publisher, 1990.
  215. de Ruiter, B., Benson, J. E., Jacobson, R. A. and J. G. Verkade, "Rectangular Planar Chelating Frameworks: Formation of Unexpected Silicon Alkoxide Isomers", Inorg. Chem. 29, 1065 (1990).
  216. Sommerer, S., Jensen, W. P. and Jacobson, R. A., "The Metal Promoted Hydration of Di-2-Pyridyl Ketone: UV-Visible Spectra of Cu(II) and Cr(III) in Aqueous Solution with Di- 2-Pyridyl Ketone and the X-ray Structure Analysis of Bis-2,2',N,N'-Bipyridyl Ketone- Hydrate Chromium(III) Chloride and Ruthenium", Inorgan. Chim. Acta. 172, 3 (1990).
  217. Miller, L. L., Jacobson, R. A., Chen, Y.-S. and Kurtz, Jr., D. M., "Structure of Hexakis(N-methylimidazole-N')ferrate(II) Tetraphenylborate", Acta Cryst. C45, 527 (1989).
  218. Schroeder, N. C., Funchess, R., Jacobson, R. A. and Angelici, R. A., "Reactions of Cp2Fe2(CO)2(μ-CO)(μ-CSR)+ Bridging-Carbyne Complexes with Nucleophiles", Organometal. 8, 521 (1989).
  219. Sheffer, G. R., Jacobson, R. A. and King, T. S., "Chemical Nature of Alkali Promoted Copper-Cobalt-Chromium Oxide Higher Alcohol Catalysts", J. of Catal. 116, 95 (1989).
  220. Glavee, G. N., Su, Yingzhong, Jacobson, R. A. and Angelici, R. J., Reactions of CpFe(CO)2(=COCH2CH2O)+, CpFe(CO)2[=C(SMe)2]+ and Related Carabene Complexes with Reducing Agents and Nucleophiles. The Structure of {CpFe(CO)2[=C(SMe)2]}PF6", Inorganica Chim. Acta 157, 73-84 (1989).
  221. Kraus, G. A., Bougie, D., Jacobson, R. A. and Su, Y.-Z., "The Urea Connection. Intramolecular Diels-Alder Reactions of Urea", J. Organic Chem. 54, 2425 (1989).
  222. Hendrixson, T. L., ter Horst, M. A. and Jacobson, R. A., "Preparation and Crystal Structure of Pyridinium Tetraiodoantimonate(III) - An Infinite Chain Structure, J. Crystal. and Spectro. Res. 20, 105 (1990).
  223. Xi, S. K., Schmidt, H., Lensink, C., Kim, S., Wintergrass, D., Daniels, L. M., Jacobson, R. A. and Verkade, J. G., "Bridgehead-Bridgehead Communication in Untransannulated ZP(ECH2CH2)3N Systems", Inorg. Chem. 29, 2214 (1990).
  224. Chen, B. H., and Jacobson, R. A., "A Robust Method for Least Squares Lattice Parameter Refinement", Powder Diffraction 5, 144 (1990).
  225. Hendrixson, T. L., ter Horst, M. A. and Jacobson, R. A., "Crystal Structure of Dipyridinium Decaiodide - An Infinite Chain Structure", Acta Cryst. C. C47, 2141 (1991).
  226. Hendrixson, T. L., Damento, M. A. and Jacobson, R. A., "Twinning Effects in the Orthorhombic Form of a Ba2YCu3O7-x Superconductor", J. Solid State Chem. 88, 201 (1990).
  227. Davis, R. V., Wintergrass, D. J., Janakiraman, M. N., Hyatt, E. M., Jacobson, R. A., Daniels, L. M., Wroblewski, A., Amma, J. Padmakumari, Das, S. K. and Verkade, J. G., "Towards Stabilizing Rectangular Pyramidal Geometries in Non-Metals: Polycyclic Phosphorus Esters", Inorg. Chem. 30, 1330 (1991).
  228. Garant, R. J., Daniels, L. M., Das, S. K., Janakiraman, M. N., Jacobson, R. A. and Verkade, J. G., "Lewis Basicity of Silatranes and the Molecular Structures of EtOSi(OCH2CH2)3N, Me2OSi(OCH2CH2)3N and CF3CO2HEtOSi(OCH2CH2)3N", J. Am. Chem. Soc. 113, 5728 (1991).
  229. Woo, L. K., Maurya, M. R., Tolppi, C. J., Jacobson, R. A. and Yang Shumei, "Synthesis and Characterization of a New Bis-Alanyl-Appended Porphyrin and its Mononuclear Cu(II), Ni(II) and Zn(II) Complexes. Crystal Structure of the Ni(II) Complex", Inorg. Chim. Acta. 182, 41 (1991).
  230. Mason, M. R., Su, Y.-Z., Jacobson, R. A. and Verkade, J. G., "Bidentate and Tridentate Coordination Modes of a Novel Bicyclic Ditertiary Phosphine Ether", Organometallics 10, 2335 (1991).
  231. Yang, S. and Jacobson, R. A., "Synthesis, Crystal Structure and Molecular Modeling of Aquo Magnesium Tetra-(methoxyphenyl)-porphyrin", Inorg. Chim. Acta 190, 129 (1991).
  232. Woo, L. K., Hays, J. A., Jacobson, R. A. and Day, C. L., "Low-Valent Titanium Porphyrin Complexes: Synthesis and Structural Characterization of the First Ti(II) Porphyrin Complex, (_2-diphenylacetylene)Titanium(octaethylporphyrin)", Organometal. 10, 2102 (1991).
  233. Rao, K. M., Day, C. L., Jacobson, R. A. and Angelici, R. J., "ν1(S)- and ν6-Coordination of Dibenzothiophene (DBT) in Cp*MCl2[ν1(S)-DBT] and Cp*M(ν6-DBT)2+ (M = Ir and Rh)", Inorg. Chem. 30, 5046 (1991).
  234. Rao, K. M., Day, C. L., Jacobson, R. A. and Angelici, R. J., "Air Oxidation of (Cp*RuCl2)n to the Oxo-bridged Complex (Cp*RuCl2)2O", Organometallics 11, 2303 (1992).
  235. Mason, M. R., Duff, C. M., Miller, L. L., Jacobson, R. A. and Verkade, J. G., "Coordination Chemistry of a New Tetratertiary Phosphine Ligand", Inorg. Chem. 31, 2746 (1992).
  236. Woo, L. K., Maurya, M. R., Jacobson, R. A., Yang, S. and S. L. Ringrose, "Mono and Dinuclear Complexes of a New Binucleating Porphyrin, α,α,5,15-bis(o-nicotinoylamidophenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin. Crystal Structures of a Mononuclear Nickel(II) Complex and a Binuclear Cu-Pt Complex", Inorg. Chem. 31, 913 (1992).
  237. Woo, L. K., Maurya, M. R., Jacobson, R. A., Yang, S. and S. L. Ringrose, "A Comparison of Two Structural Forms of α,α,5,15-bis(o-nicotinoylamidophenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrinato Nickel(II)", Inorgan. Chim. Acta. 193, 143 (1992).
  238. Chen, J., Su, Y.-Z., Jacobson, R. A. and Angelici, R. J., "Hydride Addition to and Reduction of Cp*Ir(ν6-BT)2+ and Cp*Ir(ν6-DBT)2+, where BT=benzo[b]thiophene and DBT = dibenzothiophene", J. Organomet. Chem. 428, 415 (1992).
  239. Tang, J.-S., Laramay, M. A. H., Young, V., Ringrose, S., Jacobson, R. A. and Verkade, J. G., "Stepwise Transannular Bond Formation Between the Bridgehead Atoms in Z- P(MeNCH2CH2)3N Systems", J. Am. Chem. Soc. 114, 3129 (1992).
  240. Seo, B.-I, Suh, I.-H., Jensen, W. P., Lewis, D. P., Wall, L. K. and Jacobson, R. A., "The Conformation of 3-endo-Arylmethylisobornyl Esters", Tetrahedron Asymmetry 3, 367 (1992).
  241. Lewis, D. L., Suh, I.-H., Jensen, W. P. and Jacobson, R. A., "Structure of the p-Nitrobenzoate Ester of 3-endo-(p-Methoxybenzyl)isoborneol", Acta Cryst. C49, 562 (1993).
  242. Day, C. L. and Jacobson, R. A., "XTALLAB and POWDER Computer Assisted Instruction of Crystallographic Methods", J. Appl. Crystal. 26, 144 (1993).
  243. Naiini, A. A., Ringrose, S., Su, Y., Jacobson, R. A. and Verkade, J. G., "Unexpected Reactivity Trend in Dialkylamino Titanatranes", Inorg. Chem. 32, 1290 (1993).
  244. Bhaduri, D., Nelson, J. H., Day, C. L., Jacobson, R. A., Solujic, L. and Milosavljevic, E. B., "Iron Promoted Intramolecular [4+2] Diels-Alder Cycloadditions of 1-Phenyl-3,4- dimethylphosphole with Selected Dieneophiles", Organometallics 11, 4069 (1992).
  245. Miller, L. L., Jacobson, R. A., Ruedenberg, K., Schwarz, W. H. E. and Niu, J. E., "Oriented Atoms Least Squares. I. Equations and Methodology", Acta Cryst. (submitted).
  246. Miller, L. L., Jacobson, R. A. and Schwarz, W. H. E., "Oriented Atoms Least Squares. II. Application to 9-tert-butylanthracene, Tetrafluoroterephthalodinitrile and 1,2,3-triazine", Acta Cryst. (submitted).
  247. Kraus, G. A., Chen, Li, and Jacobson, R. A., "Synthesis and Evaluation of a Pleurotin Analog, Synth. Commun. 23, 2041 (1993).
  248. Bhaduri, D., Nelson, J. H., Day, C. L., Jacobson, R. A., Solujic, L., Milosavljevic, E. B. and Gray, G. A., π-Facial Selectivities in the Coordination of an Optically Pure Fused Cyclopentadienyl Ligand to Arene Ruthenium Moieties. Complete Spectral and Structural Characterization of a Single Diastereomer of [(PCp)Ru(Me6V6)]PF6", Inorg. Chim. Acta 221, 41 (1994).
  249. Woo, L. K., Maurya, M. R., Jacobson, R. A. and Ringrose, S. L., "Synthesis, Characterization, and X-ray Crystal Structure of a Trimetallic Diporphyrin Complex", Inorg. Chim. Acta 212, 337 (1993).
  250. Day, C. L. and Jacobson, R. A., "Combining Molecular Mechanics and X-ray Diffraction Methods", The Rigaku Journal 10, 9 (1993).
  251. Sommerer, S. O., Baker, J. D., Jensen, W. P., Hamza, A. and Jacobson, R. A., "The X-ray Structure Analysis of Bis-2,2',N,N'-Bipyridyl Ketone Cobalt(III) Nitrate Dihydrate", Inorg. Chim. Acta 210, 173 (1993).
  252. Bhaduri, D., Nelson, J. H., Wang, T. and Jacobson, R. A., "Synthesis and Reactions of Iron and Ruthenium Complexes of an Optically Pure Fused Cyclopentadienyl Ligand", Organometallics, 13, 2291 (1994).
  253. Pinkas, J., Wang, T., Jacobson, R. A. and Verkade, J. G., "Azaalumatranes Exhibiting Unusual Coordination Geometries for the Aluminum", Inorg. Chem. 33, 4202 (1994).
  254. Pinkas, J., Wang, T., Jacobson, R. A. and Verkade, J. G., "Group 13 Azatranes: Structure and Reactivity", Inorg. Chem. 33, 5244 (1994).
  255. Robertson, M. J., Day, C. L., Jacobson, R. A. and Angelici, R. J., "Synthesis and Protonation of the Bridging Benzo[b]thiophene (BT) Complexes [Cp'(CO)2Re](ν2:ν1(S)μ2-BT)[Re(CO)2Cp"]", Organometallics 13, 179 (1994).
  256. Brandenburg, R. A., Ringrose, S. L. and Jacobson, R. A., "Crystal Structure of an Iodine Phenazine Complex: C12H9N2+·I3-·C12H8N2·1/6I2", J. Iowa Acad. Sci., 101, 35 (1994).
  257. Hendrixson, T. L. and Jacobson, R. A., "Locating Symmetry Elements in Patterson Superposition Maps", Zeitschrift für Kristallographie 212, 577 (1997).
  258. White, C. J., Wang, T., Jacobson, R. A. and Angelici, R. J., "Synthesis, Equilibrium Binding and 77Se NMR Studies of _1-Selenophene (Seln) Complexes: [CpRu(CO)(PPh3)(ν1(Se)-Seln)]BF4", Organometallics 13, 4474 (1994).
  259. Chen, J., Su, Y., Jacobson, R. A. and Angelici, R. J., "Reactions of the ν5-2,5-Dimethylthiophene Complex, Cp*Ir(ν5-2,5-Me2T)2+ with Nucleophiles (Ph-,Me-,-CH(CO2Me)2, and OH-)", J. Organometal. Chem. 512, 149 (1996).
  260. Zavalij, P., Guo, J.-D., Whittingham, M. S., Jacobson, R. A., Pecharsky, V., Bucher, C. K. and Hwu, S.-J., "Keggin Cluster Formation by Hydrothermal Reaction of Tungsten Trioxide with Methyl Substituted Ammonium. The Crystal Structure of Two Novel Compounds: [NH2(CH3)2]6H2W12O40·~4H2O and [N(CH3)4]6H2W12O40·2H2O", J. Solid State Chem. 123, 83 (1996).
  261. Zavalij, P. Y., Whittingham, M. S., Boylan, E. A., Pecharsky, V. K. and Jacobson, R. A., "Crystal Structure of Tetramethylammonium Tetravanadiumdecaoxide", Zeitschrift für Kristallographie 211, 464 (1996).
  262. Jensen, W. P., Hamza, A. I., Suh, I.-H., Jacobson, R. A. and Sommerer, S., "The Crystal and Molecular Structure of [2,2-N,N'-O-Bipyridyl Ketone Hydrate, N,N Bipyridylketone Oxime, Nitrito Cobalt(III)]", Inorg. Chim. Acta 254, 367 (1997) .
  263. Chen, J., Day, C. L., Jacobson, R. A. and Angelici, R. J., "Unexpected Products Resulting from Reactions of Cp*Ir(ν4-2,5-Me2T)2+ (Me2T = 2,5-dimethylthiophene) with (μ-CO)(μ-RS)Fe2(CO)6-", J. Organometal. Chem. 522, 21, (1996).
  264. Norton, G. A., Peters, R. E. and Jacobson, R. A., "Feasibility of Using X-ray Diffraction for On-Line Analysis of Gypsum During Wall Board Manufacturing", Technical Note, Min. Engineering, 8, No. 9, 1069 (1995).
  265. Jacobson, R. A., "A Cosine Transform Approach to Indexing", Zeitschrift für Kristallographie 212, 99 (1997).
  266. Wang, D., Angelici, R. J., Thomas, L. M. and Jacobson, R. A., "Crystal Structure of Carbonyl[tri(p-Chlorophenyl)phosphine] [ν5-Pentamethyl Cyclopentadienyl) Iridium(I), (CO)[p-ClC6H4)3P][ν5-C5(CH3)5]Ir", Zeitschrift für Kristallographie, 212, 245 (1997).
  267. Yokota, Y., Setterdahl, A. T., Ringrose, S., Jacobson, R. A. and Verkade, J. G., "Synthesis of Alkali and Alkaline Earth Metal Complexes of Open Cryptands", Inorg. Chem., (submitted).
  268. Jacobson, R. A., "A Monte Carlo Method for Indexing", Zeitschrift für Kristallographie, 212, 689 (1997).
  269. Jensen, W. P., Gehrke, H., Jones, D. R., Suh, I.-H. and Jacobson, R. A., "Crystal Structure of Methylene bis(triphenylphosphonium)tetrachloroferrate(III) Dihydrate, (C37H43P2)(FeCl4)2·2H2O", Zeitschrift für Kristallographie, 211, 829 (1996).
  270. Mohan, T., Arumugam, S., Wang, T., Jacobson, R. A. and Verkade, J. G., "Reactions of P(MeNCH2CH2)3N with Primary, Secondary, and Tertiary Alkyl Halides: Evidence for a Solvent-Enhanced Dehydrohalogenation", Heteroatom Chem., 7, 455 (1996).
  271. Zavalij, P. Y., Whittingham, M. S., Chirayil, T., Pecharsky, V. K. and Jacobson, R. A., "A New Decavanadate with Mixed Cations, [Li(H2O)4]2[N(C3)4]4[V10O28]·4H2O", Acta Crystallogr. C53, 170 (1997).
  272. Boever, C., Gislason, J., Jensen, Wm. P. and Jacobson, R. A., "Ab Initio Calculations and X-ray Structure Determinations of Dichloro(O-O'-O"-1,3,5-cyclohexanetriol)Copper(II) and bis(O-O'O"-1,3,5-hexanetriol)Nickel(II)", Inorg. Chim. Acta. (accepted).
  273. Jacobson, R. A., "Single Crystal X-ray Structure Determination", Book Chapter in Methods in Materials Research, in press.